Structures by: Chauvin R.

Total: 59

C47H28Cl2F6O2

C47H28Cl2F6O2

Rives, ArnaudBaglai, IaroslavBarthes, CécileMaraval, ValérieSaffon-Merceron, NathalieSaquet, AlixVoitenko, ZoiaVolovenko, YulianChauvin, Remi

Chem. Sci. (2015) 6, 2 1139

a=12.5119(17)Å   b=12.6648(17)Å   c=14.9565(19)Å

α=70.805(5)°   β=66.621(5)°   γ=67.665(5)°

C49H25Cl3F12O2

C49H25Cl3F12O2

Rives, ArnaudBaglai, IaroslavBarthes, CécileMaraval, ValérieSaffon-Merceron, NathalieSaquet, AlixVoitenko, ZoiaVolovenko, YulianChauvin, Remi

Chem. Sci. (2015) 6, 2 1139

a=12.8182(16)Å   b=35.815(5)Å   c=9.7626(14)Å

α=90.00°   β=92.841(6)°   γ=90.00°

C48H30F6O4

C48H30F6O4

Rives, ArnaudBaglai, IaroslavBarthes, CécileMaraval, ValérieSaffon-Merceron, NathalieSaquet, AlixVoitenko, ZoiaVolovenko, YulianChauvin, Remi

Chem. Sci. (2015) 6, 2 1139

a=13.07527(8)Å   b=16.18867(10)Å   c=19.01027(12)Å

α=90°   β=100.1002(6)°   γ=90°

C130H174O6

C130H174O6

Zhu, ChongweiWang, Tsai-HuiSu, Chien-JhangLee, Shern-LongRives, ArnaudDuhayon, CarineKauffmann, BriceMaraval, ValérieCHEN, Chun-hsienHsu, Hsiu-FuChauvin, Remi

Chem. Commun. (2017)

a=49.45(2)Å   b=15.293(11)Å   c=7.3526(14)Å

α=90°   β=91.49(3)°   γ=90°

C70H62,2(CHCl3)

C70H62,2(CHCl3)

Zhu, ChongweiDuhayon, CarineRomero-Borja, DanielMaldonado, Jose-LuisRamos-Ortiz, GabrielSaquet, AlixMaraval, ValérieChauvin, Remi

New J. Chem. (2017)

a=10.1720(5)Å   b=11.8006(8)Å   c=12.8576(7)Å

α=90.105(5)°   β=101.559(5)°   γ=94.484(5)°

C54H30,CHCl3

C54H30,CHCl3

Zhu, ChongweiDuhayon, CarineRomero-Borja, DanielMaldonado, Jose-LuisRamos-Ortiz, GabrielSaquet, AlixMaraval, ValérieChauvin, Remi

New J. Chem. (2017)

a=12.4948(5)Å   b=16.0972(6)Å   c=20.2765(9)Å

α=90°   β=90°   γ=90°

C16H17N4O1P1

C16H17N4O1P1

Maaliki, CarineCanac, YvesLepetit, ChristineDuhayon, CarineChauvin, Remi

RSC Advances (2013) 3, 43 20391

a=15.4580(3)Å   b=9.54826(16)Å   c=20.4320(4)Å

α=90°   β=90°   γ=90°

C18H23N4P,2(CF3O3S)

C18H23N4P,2(CF3O3S)

Maaliki, CarineCanac, YvesLepetit, ChristineDuhayon, CarineChauvin, Remi

RSC Advances (2013) 3, 43 20391

a=15.7038(3)Å   b=25.3224(3)Å   c=13.7018(2)Å

α=90°   β=107.6226(18)°   γ=90°

C18H23N4OP,2(CF3O3S),C2H3N

C18H23N4OP,2(CF3O3S),C2H3N

Maaliki, CarineCanac, YvesLepetit, ChristineDuhayon, CarineChauvin, Remi

RSC Advances (2013) 3, 43 20391

a=10.2649(3)Å   b=12.1611(4)Å   c=12.7816(4)Å

α=81.178(2)°   β=71.935(2)°   γ=72.878(2)°

C10H11N2O4P,C2H5NO

C10H11N2O4P,C2H5NO

Gao, MingLi, YiXie, LijuanChauvin, RemiCui, Xiuling

Chemical communications (Cambridge, England) (2016) 52, 13 2846-2849

a=7.6832(6)Å   b=9.6923(7)Å   c=10.0668(9)Å

α=89.063(6)°   β=82.389(7)°   γ=80.144(7)°

C32H28P2,2(CF3O3S)

C32H28P2,2(CF3O3S)

Abdalilah, MohammedZurawinski, RemigiuzCanac, YvesLaleu, BenoîtLacour, JérômeLepetit, ChristineMagro, GerminalBernardinelli, GéraldDonnadieu, BrunoDuhayon, CarineMikolajczyk, MarianChauvin, Remi

Dalton Transactions (2009) 40 8493-8508

a=9.5353(9)Å   b=19.6190(13)Å   c=19.8829(18)Å

α=90°   β=99.024(11)°   γ=90°

C32H29OP2,C4H8O,F6P

C32H29OP2,C4H8O,F6P

Abdalilah, MohammedZurawinski, RemigiuzCanac, YvesLaleu, BenoîtLacour, JérômeLepetit, ChristineMagro, GerminalBernardinelli, GéraldDonnadieu, BrunoDuhayon, CarineMikolajczyk, MarianChauvin, Remi

Dalton Transactions (2009) 40 8493-8508

a=11.474(5)Å   b=12.913(5)Å   c=13.705(5)Å

α=110.218(5)°   β=113.218(5)°   γ=91.949(5)°

C19H18P,C18Cl12O6P

C19H18P,C18Cl12O6P

Abdalilah, MohammedZurawinski, RemigiuzCanac, YvesLaleu, BenoîtLacour, JérômeLepetit, ChristineMagro, GerminalBernardinelli, GéraldDonnadieu, BrunoDuhayon, CarineMikolajczyk, MarianChauvin, Remi

Dalton Transactions (2009) 40 8493-8508

a=17.6833(9)Å   b=17.6833(9)Å   c=11.4829(5)Å

α=90.00000°   β=90.00000°   γ=120.0000°

C35H34P2,2(CF3O3S),1.5(CH2Cl2)

C35H34P2,2(CF3O3S),1.5(CH2Cl2)

Abdalilah, MohammedZurawinski, RemigiuzCanac, YvesLaleu, BenoîtLacour, JérômeLepetit, ChristineMagro, GerminalBernardinelli, GéraldDonnadieu, BrunoDuhayon, CarineMikolajczyk, MarianChauvin, Remi

Dalton Transactions (2009) 40 8493-8508

a=35.0471(11)Å   b=14.8261(5)Å   c=17.1363(6)Å

α=90°   β=103.455(3)°   γ=90°

C32H30P2,2(CF3O3S),2(C0.80H1.20O0.40),H2O

C32H30P2,2(CF3O3S),2(C0.80H1.20O0.40),H2O

Abdalilah, MohammedZurawinski, RemigiuzCanac, YvesLaleu, BenoîtLacour, JérômeLepetit, ChristineMagro, GerminalBernardinelli, GéraldDonnadieu, BrunoDuhayon, CarineMikolajczyk, MarianChauvin, Remi

Dalton Transactions (2009) 40 8493-8508

a=10.799(2)Å   b=12.013(2)Å   c=15.743(3)Å

α=90.00°   β=97.25(3)°   γ=90.00°

C41H39N3PPd,CF3O3S,CH2Cl2

C41H39N3PPd,CF3O3S,CH2Cl2

Abdellah, IbrahimDebono, NathalieCanac, YvesDuhayon, CarineChauvin, Remi

Dalton Transactions (2009) 35 7196

a=12.2369(2)Å   b=16.1127(3)Å   c=20.5946(4)Å

α=90°   β=90°   γ=90°

C31H25Cl2N2PPd

C31H25Cl2N2PPd

Abdellah, IbrahimDebono, NathalieCanac, YvesDuhayon, CarineChauvin, Remi

Dalton Transactions (2009) 35 7196

a=11.5754(9)Å   b=20.3835(17)Å   c=26.4657(19)Å

α=90°   β=90.148(3)°   γ=90°

C34H31ClN2PPd,CF3O3S,CH2Cl2

C34H31ClN2PPd,CF3O3S,CH2Cl2

Abdellah, IbrahimDebono, NathalieCanac, YvesDuhayon, CarineChauvin, Remi

Dalton Transactions (2009) 35 7196

a=11.1808(10)Å   b=18.1687(12)Å   c=18.3719(13)Å

α=90°   β=90°   γ=90°

C41H39N3PPd,CF3O3S,(H2O)

C41H39N3PPd,CF3O3S,(H2O)

Abdellah, IbrahimDebono, NathalieCanac, YvesDuhayon, CarineChauvin, Remi

Dalton Transactions (2009) 35 7196

a=12.4645(4)Å   b=15.7229(4)Å   c=20.4721(6)Å

α=90°   β=90°   γ=90°

C33H30P2,C3H6O,2(I)

C33H30P2,C3H6O,2(I)

Abdalilah, MohammedZurawinski, RemigiuzCanac, YvesLaleu, BenoîtLacour, JérômeLepetit, ChristineMagro, GerminalBernardinelli, GéraldDonnadieu, BrunoDuhayon, CarineMikolajczyk, MarianChauvin, Remi

Dalton Transactions (2009) 40 8493-8508

a=16.1216(9)Å   b=16.4811(14)Å   c=26.8178(15)Å

α=90°   β=101.602(7)°   γ=90°

C31H25Cl2N2PPd,2(CH2Cl2)

C31H25Cl2N2PPd,2(CH2Cl2)

Abdellah, IbrahimDebono, NathalieCanac, YvesDuhayon, CarineChauvin, Remi

Dalton Transactions (2009) 35 7196

a=12.6431(4)Å   b=12.0659(4)Å   c=22.2303(8)Å

α=90°   β=91.664(2)°   γ=90°

C56H64N2Si2

C56H64N2Si2

Remi ChauvinArnaud RivesIaroslav BaglaiVolodymyr MalytskyiValerie MaravalNathalie SaffonZoia Voitenko

Chem.Commun. (2012) 48, 8763

a=7.4967(6)Å   b=7.7637(7)Å   c=21.2257(17)Å

α=97.551(4)°   β=93.735(4)°   γ=96.544(4)°

C60H72N2Si2

C60H72N2Si2

Remi ChauvinArnaud RivesIaroslav BaglaiVolodymyr MalytskyiValerie MaravalNathalie SaffonZoia Voitenko

Chem.Commun. (2012) 48, 8763

a=9.2348(9)Å   b=9.3293(9)Å   c=15.6051(16)Å

α=104.252(5)°   β=91.728(4)°   γ=95.653(4)°

C54.5H33ClN2

C54.5H33ClN2

Remi ChauvinArnaud RivesIaroslav BaglaiVolodymyr MalytskyiValerie MaravalNathalie SaffonZoia Voitenko

Chem.Commun. (2012) 48, 8763

a=12.456(4)Å   b=16.127(5)Å   c=20.503(7)Å

α=90.00°   β=90.00°   γ=90.00°

C74H48N2

C74H48N2

Baglai, IaroslavMaraval, ValérieBijani, ChristianSaffon-Merceron, NathalieVoitenko, ZoiaVolovenko, Yulian M.Chauvin, Remi

Chemical Communications (Cambridge, United Kingdom) (2013) 49, 75 8374-8376

a=9.095(2)Å   b=26.610(7)Å   c=11.307(3)Å

α=90.00°   β=110.389(14)°   γ=90.00°

C79.5H51.5Cl6.5N2

C79.5H51.5Cl6.5N2

Baglai, IaroslavMaraval, ValérieBijani, ChristianSaffon-Merceron, NathalieVoitenko, ZoiaVolovenko, Yulian M.Chauvin, Remi

Chemical Communications (Cambridge, United Kingdom) (2013) 49, 75 8374-8376

a=12.939(6)Å   b=15.040(7)Å   c=18.094(8)Å

α=80.329(19)°   β=78.847(18)°   γ=74.329(18)°

1,1'-(1,2-Phenylene)bis(3-methyl-1<i>H</i>-imidazol-3-ium) bis(trifluoromethanesulfonate)

C14H16N42,2(CF3O3S)

Duhayon, CarineCanac, YvesDubrulle, LaurentMaaliki, CarineChauvin, Remi

Acta Crystallographica Section C (2016) 72, 3 198-202

a=11.37505(13)Å   b=16.09785(17)Å   c=11.60677(14)Å

α=90°   β=96.0475(11)°   γ=90°

1-Ethyl-2-phenyl-3-[2-(trimethylsilyl)ethynyl]-1<i>H</i>-indole

C21H23N1Si1

Baglai, IaroslavMaraval, ValérieDuhayon, CarineChauvin, Remi

Acta Crystallographica Section E (2013) 69, 6 o921-o922

a=12.6271(6)Å   b=9.3928(5)Å   c=16.6616(8)Å

α=90°   β=111.954(2)°   γ=90°

C31H54N4P,BF4

C31H54N4P,BF4

Mboyi, Clève DionelPoater, AlbertPoater, JordiDuhayon, CarineChauvin, Remi

The Journal of organic chemistry (2020)

a=14.3278(8)Å   b=16.4010(9)Å   c=28.7615(16)Å

α=90°   β=90°   γ=90°

C50H38,CH2Cl2

C50H38,CH2Cl2

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=13.0609(14)Å   b=14.0494(16)Å   c=22.454(3)Å

α=77.832(3)°   β=75.363(3)°   γ=85.051(3)°

C50.67H39.33Cl1.33

C50.67H39.33Cl1.33

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=16.195(2)Å   b=19.407(3)Å   c=20.992(3)Å

α=69.639(4)°   β=68.618(4)°   γ=82.046(4)°

C62H62,2(CH2Cl2)

C62H62,2(CH2Cl2)

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=10.7200(5)Å   b=45.197(2)Å   c=12.0719(5)Å

α=90°   β=114.6957(14)°   γ=90°

C46H30

C46H30

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=16.8971(10)Å   b=6.0972(4)Å   c=16.0454(10)Å

α=90°   β=106.6094(17)°   γ=90°

C70H78

C70H78

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=18.391(3)Å   b=5.5876(9)Å   c=26.892(5)Å

α=90°   β=90.190(6)°   γ=90°

C58H54,CHCl3

C58H54,CHCl3

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=13.1786(5)Å   b=13.3182(5)Å   c=14.4208(6)Å

α=92.0053(16)°   β=110.5356(15)°   γ=91.6484(16)°

C82H102,2(CH2Cl2)

C82H102,2(CH2Cl2)

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=12.3283(9)Å   b=17.5410(13)Å   c=18.7671(13)Å

α=70.412(2)°   β=89.193(2)°   γ=70.980(2)°

C82H102,2(CHCl3)

C82H102,2(CHCl3)

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=10.5493(7)Å   b=12.2119(8)Å   c=16.3716(12)Å

α=76.044(4)°   β=78.422(4)°   γ=64.554(3)°

C49.05Cl0.42F21.89O0.21

C49.05Cl0.42F21.89O0.21

Zhu, ChongweiRives, ArnaudDuhayon, CarineMaraval, ValérieChauvin, Remi

The Journal of organic chemistry (2017) 82, 2 925-935

a=14.7492(5)Å   b=30.0592(10)Å   c=47.2671(14)Å

α=90°   β=94.950(3)°   γ=90°

C13H14NO4

C13H14NO4

Yu, YunliangKuai, ChangshengChauvin, RemiTian, NianMa, ShuangshuangCui, Xiuling

The Journal of organic chemistry (2017) 82, 16 8611-8616

a=7.9578(3)Å   b=14.6936(5)Å   c=24.4705(10)Å

α=90°   β=97.184(3)°   γ=90°

C20H26O2

C20H26O2

Listunov, DymytriiFabing, IsabelleSaffon-Merceron, NathalieGaspard, HafidaVolovenko, YulianMaraval, ValérieChauvin, RemiGénisson, Yves

The Journal of organic chemistry (2015) 80, 11 5386-5394

a=4.5889(2)Å   b=46.758(2)Å   c=8.8264(5)Å

α=90°   β=104.958(3)°   γ=90°

C40H63NO2Si

C40H63NO2Si

Listunov, DymytriiFabing, IsabelleSaffon-Merceron, NathalieGaspard, HafidaVolovenko, YulianMaraval, ValérieChauvin, RemiGénisson, Yves

The Journal of organic chemistry (2015) 80, 11 5386-5394

a=23.139(5)Å   b=7.1275(15)Å   c=23.454(5)Å

α=90°   β=96.439(7)°   γ=90°

(C28H36P)2,(C18Cl12O6P)4,C6H14,(C4H8O2)1.5

(C28H36P)2,(C18Cl12O6P)4,C6H14,(C4H8O2)1.5

Benoît LaleuGérald BernardinelliRemi ChauvinJérôme Lacour

Journal of Organic Chemistry (2006) 71, 7412-7416

a=12.3799(5)Å   b=24.2382(12)Å   c=21.2644(10)Å

α=90.00000°   β=101.707(5)°   γ=90.00000°

[1,8-Bis(diphenylphosphanyl)naphthalene]dihydroboron Hexafluorophosphate

C34H28BP2,F6P,CH2Cl2

Owsianik, KrzysztofChauvin, RemiBalińska, AgnieszkaWieczorek, MichałCypryk, MarekMikołajczyk, Marian

Organometallics (2009) 28, 17 4929

a=11.964(3)Å   b=12.191(3)Å   c=12.717(3)Å

α=70.72(3)°   β=85.66(3)°   γ=72.35(3)°

C25H21N2O2PRh,CF3O3S

C25H21N2O2PRh,CF3O3S

Yves CanacChristine LepetitMohammed AbdalilahCarine DuhayonRemi Chauvin

Journal of the American Chemical Society (2008) 130, 8406-8413

a=10.9475(9)Å   b=15.1007(10)Å   c=16.0585(13)Å

α=90°   β=91.497(10)°   γ=90°

C31H34ClN2PRh,CF3O3S

C31H34ClN2PRh,CF3O3S

Yves CanacChristine LepetitMohammed AbdalilahCarine DuhayonRemi Chauvin

Journal of the American Chemical Society (2008) 130, 8406-8413

a=9.8451(8)Å   b=11.9474(12)Å   c=16.0624(15)Å

α=82.894(12)°   β=84.034(11)°   γ=78.412(11)°

C36H28N4P2

C36H28N4P2

Cécile BarthesChristine LepetitYves CanacCarine DuhayonDavit ZargarianRemi Chauvin

Inorganic Chemistry (2013) 52, 48-58

a=10.1714(8)Å   b=20.5363(13)Å   c=15.1935(9)Å

α=90°   β=109.556(3)°   γ=90°

C38H34N4P2,2(CF3O3S)

C38H34N4P2,2(CF3O3S)

Cécile BarthesChristine LepetitYves CanacCarine DuhayonDavit ZargarianRemi Chauvin

Inorganic Chemistry (2013) 52, 48-58

a=15.633(3)Å   b=22.942(5)Å   c=14.911(3)Å

α=90°   β=116.15(3)°   γ=90°

C39H34ClN4OP2Rh,2(CF3O3S)

C39H34ClN4OP2Rh,2(CF3O3S)

Cécile BarthesChristine LepetitYves CanacCarine DuhayonDavit ZargarianRemi Chauvin

Inorganic Chemistry (2013) 52, 48-58

a=12.7519(12)Å   b=13.7106(13)Å   c=13.8297(13)Å

α=77.390(4)°   β=79.713(4)°   γ=68.869(4)°

C16H17N4P1

C16H17N4P1

Maaliki, CarineCanac, YvesLepetit, ChristineDuhayon, CarineChauvin, Remi

RSC Advances (2013) 3, 43 20391

a=11.3573(2)Å   b=12.6287(3)Å   c=10.6515(2)Å

α=90°   β=90°   γ=90°

C16H14N4O2Rh,CF3O3S,2(CH2Cl2)

C16H14N4O2Rh,CF3O3S,2(CH2Cl2)

Yves CanacChristine LepetitMohammed AbdalilahCarine DuhayonRemi Chauvin

Journal of the American Chemical Society (2008) 130, 8406-8413

a=13.5516(5)Å   b=11.7085(4)Å   c=16.9923(6)Å

α=90°   β=90°   γ=90°

C36H28N4P2

C36H28N4P2

Yves CanacNathalie DebonoChristine LepetitCarine DuhayonRemi Chauvin

Inorganic Chemistry (2011) 50, 10810-10819

a=49.677(3)Å   b=8.5858(5)Å   c=14.3598(9)Å

α=90°   β=94.008(3)°   γ=90°

C38H34N4P2,2(CF3O3S)

C38H34N4P2,2(CF3O3S)

Yves CanacNathalie DebonoChristine LepetitCarine DuhayonRemi Chauvin

Inorganic Chemistry (2011) 50, 10810-10819

a=30.774(3)Å   b=12.2594(14)Å   c=28.281(3)Å

α=90°   β=105.148(4)°   γ=90°

C37H31Cl2N4P2Pd,CF3O3S,3(H2O)

C37H31Cl2N4P2Pd,CF3O3S,3(H2O)

Yves CanacNathalie DebonoChristine LepetitCarine DuhayonRemi Chauvin

Inorganic Chemistry (2011) 50, 10810-10819

a=9.3420(4)Å   b=26.2671(8)Å   c=17.4220(5)Å

α=90°   β=93.916(5)°   γ=90°

C38H34Cl2N4P2Pd,2(CF3O3S),2(C2H3N)

C38H34Cl2N4P2Pd,2(CF3O3S),2(C2H3N)

Yves CanacNathalie DebonoChristine LepetitCarine DuhayonRemi Chauvin

Inorganic Chemistry (2011) 50, 10810-10819

a=16.8049(4)Å   b=16.7864(4)Å   c=17.5998(5)Å

α=90°   β=103.697(3)°   γ=90°

C78H68Ag2F6N8O6P4S2,4(CF3O3S),8(CH2Cl2)

C78H68Ag2F6N8O6P4S2,4(CF3O3S),8(CH2Cl2)

Canac, YvesBijani, ChristianDuhayon, CarineChauvin, Remi

Organometallics (2013) 32, 15 4054

a=12.9966(6)Å   b=15.1948(7)Å   c=17.7641(8)Å

α=112.089(2)°   β=91.984(2)°   γ=112.300(2)°

C14H10Co2O10

C14H10Co2O10

Soleilhavoup, MichèleSaccavini, CatherineLepetit, ChristineLavigne, GuyMaurette, LucDonnadieu, BrunoChauvin, Remi

Organometallics (2002) 21, 5 871

a=9.222(2)Å   b=9.347(2)Å   c=12.697(3)Å

α=73.30(3)°   β=87.57(3)°   γ=62.87(3)°

C21H10CoO13

C21H10CoO13

Soleilhavoup, MichèleSaccavini, CatherineLepetit, ChristineLavigne, GuyMaurette, LucDonnadieu, BrunoChauvin, Remi

Organometallics (2002) 21, 5 871

a=7.515(2)Å   b=10.637(2)Å   c=16.180(3)Å

α=94.56(3)°   β=94.54(3)°   γ=92.04(3)°

C13H5ClO9Ru3

C13H5ClO9Ru3

Soleilhavoup, MichèleSaccavini, CatherineLepetit, ChristineLavigne, GuyMaurette, LucDonnadieu, BrunoChauvin, Remi

Organometallics (2002) 21, 5 871

a=9.443(2)Å   b=9.501(2)Å   c=10.194(2)Å

α=77.43(3)°   β=87.03(3)°   γ=86.13(3)°